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(14)制备Fmoc-Glu(otBu)-Pro-Pro-Pro-Gly-Lys(Boc)-Pro-Ala-Asp(otBu)-Asp(otBu)-Ala-Gly-Leu-Val-树脂： (14) Preparation of Fmoc-Glu(otBu)-Pro-Pro-Pro-Gly-Lys(Boc)-Pro-Ala-Asp(otBu)-Asp(otBu)-Ala-Gly-Leu-Val-resin: 在步骤(13)的Fmoc-Pro-Pro-Pro-Gly-Lys(Boc)-Pro-Ala-Asp(otBu)-Asp(otBu)-Ala-Gly-Leu-Val-树脂中，加入脱帽试剂10～50℃反应5～30分钟，用真空泵抽干，重新加入脱帽试剂10～50℃反应10～60分钟，抽干，用异丙醇洗涤3次，DMF洗涤3次，重蒸过的DMF洗涤2次，加入用DMF溶解的Fmoc-Glu(otBu)-OH、DIEA、TBTU/HOBt或HBTU/HOBt或BOP/HOBt的混合物，10～50℃反应10～60分钟，用真空泵抽干，用异丙醇洗涤3次，DMF洗涤3次，重蒸过的DMF洗涤2次，抽干，获得Fmoc-Glu(otBu)-Pro-Pro-Pro-Gly-Lys(Boc)-Pro-Ala-Asp(otBu)-Asp(otBu)-Ala-Gly-Leu-Val-树脂； In the Fmoc-Pro-Pro-Pro-Gly-Lys(Boc)-Pro-Ala-Asp(otBu)-Asp(otBu)-Ala-Gly-Leu-Val-resin of step (13), add decapping reagent 10 React at ~50°C for 5-30 minutes, drain with a vacuum pump, re-add capping reagent at 10-50°C, react for 10-60 minutes, drain, wash with isopropanol for 3 times, DMF for 3 times, and distilled DMF Twice, add the mixture of Fmoc-Glu(otBu)-OH, DIEA, TBTU/HOBt or HBTU/HOBt or BOP/HOBt dissolved in DMF, react at 10-50°C for 10-60 minutes, dry with a vacuum pump, and use iso Propanol was washed 3 times, DMF was washed 3 times, the DMF that redistilled was washed 2 times, was sucked dry, obtained Fmoc-Glu(otBu)-Pro-Pro-Pro-Gly-Lys(Boc)-Pro-Ala-Asp( otBu)-Asp(otBu)-Ala-Gly-Leu-Val-resin https://lookaside.instagram.com/seo/google_widget/crawler/?media_id=3824096370157046863 diy-serum-booster-icon Duration:90 day supply (6 packages) Glutathione is a powerful antioxidant that has many benefits for your overall health. But did you know it can help clear up acne? Glutathione helps remove harmful toxins from the body like pollutants, ...